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Re: A simple way to MAKE x-rays????
I have attached a file that I came across a
couple of years ago -- perhaps it will be of
some interest to you.
Cary
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Cary Renquist crenquis@goldengate.net
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htt v. 1997-05-08
Extracted from TV.tube.to.Xray.tube.html, 4 Aug 1997, 21:57
Generating X-Rays with Receiving Tubes
------------------------------------------------------------------------
This article, which describes the experiments of Bob Templeman of
Chicago, IL, is from the Bell Jar (electronic version) No. 2 (October
1994), which was condensed from material originally presented in Volume
3, Numbers 1 ? 2 (Winter ? Spring 1994) of the Bell Jar . Full
circuit schematics as well as sample radiographs are presented in the
original articles. Devoted to the vacuum experimenter, the intent of
the Bell Jar is to broaden interest in vacuum technology through
useful discussions of theory and technique, and to present ways in
which a variety of apparatus may be assembled using common and
inexpensive materials. Information on the Bell Jar may be obtained by
sending email to the editor, Steve Hansen, at hansen35@delphi.com or by
writing to 35 Windsor Dr., Amherst, NH 03031. New numbers will be
mailed at approx. quarterly intervals. Email subscriptions are free and
may be obtained by contacting the editor. Comments, contributions and
criticisms are always welcome. Copyright 1994, Stephen P. Hansen. ;
------------------------------------------------------------------------
Introduction: Cold and Hot Cathode X-Ray Tubes
The earliest x-ray tubes were of the cold cathode variety. These tubes,
referred to as Crookes or Hittorf tubes, were of the general class of
gas tubes since the pressure had to be in the `soft' vacuum range
(about 10-3 to 10-4 Torr) to permit the passage of electrons from the
cathode to the x-ray producing target in a so-called `dark' discharge.
Higher pressures would result in a luminous discharge (as in a neon
lamp) with only a small potential drop across the tube. Lower pressures
(a `hard' vacuum) would result in no current flow regardless of applied
voltage.
The cold cathode tube went out of use shortly after 1910 when W. D.
Coolidge introduced a tube with a hot cathode (thermionic) electron
emitter. The Coolidge tube, which uses high vacuum (i.e. below 10-5
Torr), has a number of advantages over the gas tube.
With the gas tube, the electron current, at a given voltage, is
dependent the voltage across the tube which, in turn, can vary
depending upon the degree of vacuum. Furthermore, the degree of vacuum
will change over time. This will affect the spectrum (hence the
penetrating quality) of the x-ray output as well as the intensity. With
a heated cathode in a high vacuum tube, the electron current may be
controlled simply by varying the filament temperature. Then, by varying
the voltage across the tube, the penetrating power of the x-rays (a
function of the x-ray energy) may be varied. Thus, two important
parameters may be controlled independently.
Using Receiving Tubes in a Cold Cathode Mode
Bob Templeman has been able to use conventional vacuum tubes as cold
cathode x-ray tubes. He has done most of his work with the 6BK4B, a
beam triode used for voltage regulation of high voltage, low current dc
power supplies in color and black-and-white television sets. The tube
has an octal base and a plate cap. Bob has also tried several other
tubes including the 6EN4 (which is very similar to the 6BK4B), 3AT2,
3CZ3A, and 3BW4. He has found that all will emit measurable amounts of
x-radiation but only the beam tubes appear to provide sufficient
radiation to expose standard films.
Since the tube is operated in a cold cathode mode, the tube's degree of
vacuum is quite important. Bob found that about one in eight tubes is
able to produce enough radiation to expose his film. One might ask "why
not just heat the filament to get an assured, controlled emission of
x-rays?" The answer lies in the basic characteristics of a high vacuum
diode. A `normal' vacuum diode, such as a rectifier tube, operates in
a region where the tube current varies nearly linearly with the voltage
drop. Thus, substantial increases in current would be required to
produce a voltage drop across the tube significant enough to produce
useful levels of x-rays. For normal tubes, the current would be well in
excess of the tube's power rating. Normal operation for a rectifier
tube is moderate to high current with a low voltage drop.
What is good for rectifiers is not good for x-ray tubes. In the case of
the x-ray tube, the tube is operated in the upper part of the
characteristic curve, the 'saturation' region. In this mode, the
voltage can be increased with little increase of electron current.
Getting the right balance between current and voltage is part of each
tube's design. Also, as noted before, varying the filament temperature
(e.g. by means of varying the filament voltage) allows the intensity of
the tube's output to be adjusted. For each filament temperature, there
is a different current vs. voltage characteristic.
The High Voltage Power Supply
Bob uses a TV flyback driven voltage multiplier to power his tubes.
This is a fairly common implementation using a pair of general purpose
NPN transistors to drive a 10 turn primary which is added to a stock
flyback.
The multiplier is of the cascade (Cockcroft-Walton) type. A modular
tripler scavenged from a TV set can be used as these can usually be
pushed to about 40 kV without failing. A better alternative is to make
the multiplier from scratch using discrete diodes and ceramic disk
capacitors. The diodes should be rated at 20 kV. A good value for the
capacitors would be 0.001 mF at 15 kV.
As the flyback circuit will provide about 10 kV into the multiplier,
six stages are required to boost the voltage to a maximum of 60 kV.
The multiplier can be assembled on a piece of bare perf board with good
separation between the components. To avoid excessive leakage or
arcing, immerse the whole multiplier assembly in mineral oil. A
rectangular plastic food storage dish makes a good container for this
assembly.
A means of measuring the high voltage output is essential. A resistive
divider is appropriate for this application. However, standard
components are not suitable for high voltages, low current
measurements. A good circuit for measuring the output voltage is a
potted TV focus divider (RCA SK series or equivalent) which contains
the necessary high voltage/high value resistors. The only additional
components needed are one external resistor and a standard high
impedance dc meter.
When testing the completed multiplier, avoid the temptation to draw
sparks from the output. This will only stress the components and lead
to premature failure.
Producing X-Rays
When all is set with the high voltage circuitry and several candidate
tubes are in hand, it is time to try generating some x-rays. First,
make sure that you have an operating x-ray monitor. This will be needed
for checking tubes for output as well as for checking the effectiveness
of the shielding. Bob uses a simple Geiger counter circuit which is
provided as a kit from Electronic Goldmine (P.O. Box 5408, Scottsdale,
AZ 85261). This kit, #C6430, which has an audio output, currently lists
for $59.95.
Bob notes that the tubes tend to operate better when the normal cathode
is positive, probably because of the slightly higher impedance in this
configuration. As this tube element is smaller, the image tends to be a
bit sharper. Still, receiving tubes are relatively diffuse emitters of
x-rays and the images will be slightly fuzzy.
X-rays are nothing to be treated casually. Bob surrounds his tubes
with 2 to 4 inches of lead. (At 60 kV, 1/16 inch of lead is the
absolute minimum.) Maintaining a dosimetry program is advisable and
some suggestions are provided later in the article. Finally, the safest
practice is to operate the tube from a remote location.
Arc-over is a problem at the voltages Bob has been using. Encasing the
tubes in wax was tried but found to be only partially effective. Bob's
prize 6EN4, the best emitter of x-rays, was destroyed in spite of this
encapsulation. Immersing the tubes in mineral oil appears to be more
effective. (Watch your druggist's face when you purchase the several
bottles of mineral oil which will be needed for insulation of the tube
and multiplier!)
Even operating in a cold cathode mode, the current through these tubes
at 40 to 60 kV is enough to cause heating. Furthermore, as the tube
elements warm up, the cathode begins to emit electrons thermionically.
This leads to increasing dissipation, lowered potential, and a shift of
the x-ray emission toward the soft, less penetrating, region of the
spectrum.
Bob supplied a number of radiographs which were printed with the
original article. These showed the internal circuitry of several potted
modules as well as the internal structure of a 308 Winchester rifle
shell.
The best radiographs taken to date have used Agfapan 400 sheet film.
Typical exposures were 30 minutes with the tube about 8.5 inches from
the film plane. With a negative bias of 40 kV applied to the plate cap,
the tubes draw about 20 microamps.
Bob has been investigating the sensitivities of various phosphors to
the x-rays emitted from his tubes. He had no luck with the phosphor
salvaged from a fluorescent light tube but he did get a faint
fluorescence from the phosphor scraped from the face of a broken color
picture tube. The brightness was about comparable to that from a piece
of standard medical rare earth phosphor x-ray intensifier screen.
Dosimetry
Any person who regularly works with any combination of high voltage and
vacuum should maintain a dosimetry program.
Landauer (2 Science Road, Glenwood, IL 60425-1586, (708) 755-7000)
provides film and thermoluminescent (TLD) dosimeters as part of their
service. These are provided as either wearable badges or as room
monitors. To sign up for the service you select a monitoring frequency
(weekly, monthly, quarterly) and pay a small set-up fee plus a year's
payment in advance. Before the end of each monitoring period, you
receive a new badge. At the end of each period you send in the current
badge and within 5 days you receive a report giving dosage for the
period plus cumulative dosage. For a TLD dosimeter sensitive to x-ray,
gamma, and beta radiation with a quarterly schedule, the cost is under
$100 for a year.
Another approach to dosimetry and one which gives a continuous record
is a Geiger counter provided by Aware Electronics (P.O. Box 4299,
Wilmington, DE 19807, (302) 655-3800). Their RM-60 is a small monitor
which interfaces directly to an IBM compatible computer via a phone
type cable to the serial or printer port. A dedicated PC is not
required as the software gathers the data and stores it to disk even
while the computer is running other applications. The software displays
the data in a scrolling bar chart format with date and time for each
bar. Also provided is the cumulative average dosage. Cost for the RM-60
package is about $150. Aware's catalog also describes several other
radiation monitoring items.
Further Reading
Using standard vacuum tubes to produce x-rays is nothing new. C. L.
Stong's "Scientific American Book of Projects for the Amateur
Scientist" (Simon and Schuster, 1960) has a chapter describing Harry
Simons's impressive experiments using antique 01 tubes driven by a
homebuilt Oudin coil. Mr. Simons also fabricated a variety of his own
tubes, simple bulbs with a sealed-in molybdenum cathode with a
magnesium target. The latter was deposited on the inside of the bulb,
opposite the cathode, and was capacitively coupled to the Oudin coil
by means of a layer of aluminum foil which was wrapped on the outside
of the bulb. Simons evacuated his tubes to 0.1 mTorr before sealing.