I agree. There are many regulations that define "clean" (e.g. MARSIMM,NUREG-5849 in the US). Typically, regulators need to be involved and approve this definition. What is clean at one site, may not be clean at another. I suggest that the requestor obtain professional consultation on this matter. I am sure that RADSAFER's will flood him with suitable recommendations.
Because gammas were specified, I believe gamma spectroscopy is the analysis of choice. However, the definition of "clean" would have to be established before choosing the analysis method.
Kevin Wright