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Reply: Sample Acidification
Jim Webb wrote in part: "We too have been wrestling with
concern about a " wall effect" -- ions in solution plating out
on the inner surface of a container."
Although the article addresses power reactor process and
effluent liquids rather than U and Pu, a good discussion of
sample preservation is in the July 1980 HP Journal. Authors
are Bernabee, Percival, and Martin, "Fractionation of
Radionuclides in Liquid Samples from Nuclear Facilities", pp
57-67.
Todd Jackson, CHP
tjj@nrc.gov
"The views expressed herein are those of the author and do
not necessarily reflect the views of NRC or the US
Government."