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RE: Measurement of Tritium by Liquid Scintillation
Radsafers:
A significant problem with measuring tritium in urine is quench.
What I do is run replicate samples by liquid scintillation 10 ul,
50 ul, 100 ul, and 1 ml of urine in 7 ml of scintillation fluid. If
they all read background, I stop there. If the readings are linear,
then quench is not a significant factor. If the readings are
nonlinear, I either take the most conservative value or spike a sample
with a known activity of tritium or both.
Running several samples of varying concentration is a quick and easy
way to evaluate whether quench is significantly affecting sample
counting.
Tom
Tom Mohaupt, MS, CHP
Wright State University
Radiation Safety Officer
Voice: (937) 775-2169
Fax: (937) 775-3301
E-mail: tmohaupt@wright.edu
Address: 104 Health Sciences Bldg, Wright State University
Dayton, OH 45435